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A bulky bidentate ligand was used to stabilize a macrocyclic [FeIII8CoII6] cluster. Tuning the basicity of the ligand by derivatization with one or two methoxy groups led to the isolation of a homologous [FeIII8CoII6] species and a [FeIII6FeII2CoIII2CoII2] complex, respectively. Lowering the reaction temperatures allowed isolation of [FeIII6FeII2CoIII2CoII2] clusters with all three ligands. Temperature‐dependent...
Identische Reaktionsgemische können, wie H. Oshio und Mitarbeiter in ihrer Zuschrift auf S. 2985 ff. zeigen, selektiv verschiedene cyanidverbrückte Heterometallcluster liefern, wenn die Labilität der Zwischenstufen über einen thermisch induzierten Elektronentransfer‐gekoppelten Spinübergang (ETCST) kontrolliert wird. Wie im Titelbild gezeigt, werden ETCST‐aktive quadratische Zwischenstufen aus einfachen...
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