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In this work, we report a facile biphasic-to-monophasic successive co-assembly approach to synthesize yolk–shell structured mesoporous organosilica nanoparticles (MONs). The yolk–shell structured MONs possess ethane-bridged frameworks, high surface area (1023m2g−1), radially oriented mesochannels (3.8nm), large pore volume (0.99cm3g−1), and tunable diameter (147–324nm) and shell thickness (23–53nm)...
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