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LiFexMn2-xO4 (x=0.0, 0.1 and 0.2) with superior rate and cycling performance is synthesized using a sol – gel method by combining citric acid and glucose as the chelating agent. For the first time Fe is found to basically occupy the 16d site. Fe doping decreases the occupancies of Mn at the 8a site considerably, and reduces the variations of the lattice volume before and after charge significantly,...
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