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An equiatomic CoCrFeNiAl high-entropy alloy was synthesized by mechanical alloying, and phase evolutions, microstructure, thermal properties and annealing behaviors were investigated. It was found that a body-centered cubic structured solid solution with refined microstructure of 20nm in grain size could be obtained after 30h milling. As-milled powder exhibited good phase stability until 500°C, and...
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