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A relay Cu(I)/Brønsted base catalyzed one‐pot phospha‐Michael addition/5‐exo‐dig cyclization/isomerization of in situ generated aza‐alkynyl o‐quinone methides (N‐o‐AQMs) from 1‐(o‐aminophenyl)prop‐2‐ynols with P(O)‐compounds has been established to afford C3‐phosphorylated indoles. It demonstrates that the 1,4‐conjugate addition adduct from N‐o‐AQMs could undergo further cyclization with the tethered...
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