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A facile solvothermal–calcining route for the large-scale synthesis of uniform β-Bi2O3 nanospheres has been demonstrated. The morphology, structure, and photoabsorption of β-Bi2O3 were characterized, and the effects of the preparation conditions on the structural properties of products were analyzed. The results show that monodisperse bismuth nanospheres are formed through the solvothermal reaction...
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