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Abstract. [Tetraamminecadmium(II)] bis(permanganate) (1) was prepared and its crystal structure was elucidated with XRD‐Rietveld refinement and vibrational spectroscopic methods. Compound 1 has a cubic lattice consisting of a 3D hydrogen‐bonded network built as four by four distorted tetrahedral blocks of [Cd(NH3)4]2+ cations and MnO4– anions, respectively. The other four permanganate ions are located...
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