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In this work, pyrazine (A), aminopyrazine (B), quinoxaline (C), and 5,6,7,8‐tetrahydroquinoxaline (D) have been screened out among a large number of pyrazine derivatives to construct Hofmann‐type metal–organic frameworks (MOFs) Fe(L)[M(CN)4] (M=Pt, Pd) with similar 3D pillared‐layer structures. X‐ray single‐crystal diffraction reveals that the alternate linkage between M and FeII ions through cyano...
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