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In this study, novel methods were used to recover the by‐product of the reaction between Al‐based composites and water for hydrogen generation as effective means to reduce the cost of hydrogen generation. The results suggest that α‐Al2O3 which is prepared from the reaction by‐product after 24 h ball milling has particle size distributions of 0.57, 1.34, and 2.865 μm for standards d10, d50, and d90...