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A novel wedge‐shaped compound containing two diacetylene tails, namely, methyl 3,5‐bis(trideca‐2,4‐diyn‐1yloxyl)benzoate (DDABM), was synthesized. As shown by UV/Vis spectroscopy this compound can be polymerized under UV irradiation. The crystalline structure of DDABM was investigated by grazing‐incidence wide‐angle X‐ray diffraction on oriented crystalline films deposited on PTFE‐rubbed silicon wafer...
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