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The partial oxidation of methane (POM) to synthesis gas over SiO2-supported Rh and Ru catalysts was studied by in situ microprobe Raman and in situ time-resolved FTIR (TR-FTIR) spectroscopies. The results of in situ microprobe Raman spectroscopic characterization indicated that no Raman band of Rh2O3 was detected at 500 °C over the Rh/SiO2 catalyst under a flow of a CH4/O2/Ar (2/1/45, molar ratio)...
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