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Transmission electron microscopy was performed on a model system of a novel CuMn2O4 spinel catalyst in order to study the effects of reduction by carbon monoxide and subsequent reoxidation by oxygen both processed at 600°C. A phase transition from CuMn2O4 spinel into separated MnO and Cu‐rich phases, which are CuO or Cu depending on the reduction period, was observed in the reduced samples. Furthermore,...
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