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FeB(C) nanocapsules were prepared by arc-discharging Fe 80 B 20 alloy in Ar and CH 4 . X-ray diffraction and transmission electron microscopy analyses showed that the FeB(C) nanocapsules had a core–shell structure with α-Fe and Fe 3 B as cores and graphite as shells. The formation mechanism of the FeB(C) nanocapsules is discussed. The graphite shells display a strong...
After carefully ruling out the known sample preparation artifacts, high-angle annular detector dark-field scanning transmission electron microscopy, nanobeam composition analysis and energy-filtered imaging suggest that phase separation occurs upon heating in the Al 85 Ni 5 Y 6 Fe 2 Co 2 amorphous ribbon prior to the onset of primary crystallization, but not...
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