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Optimizing the coordination structure and microscopic reaction environment of isolated metal sites is promising for boosting catalytic activity for electrocatalytic CO2 reduction reaction (CO2RR) but is still challenging to achieve. Herein, a newly electrostatic induced self‐assembly strategy for encapsulating isolated Ni‐C3N1 moiety into hollow nano‐reactor as I‐Ni SA/NHCRs is developed, which achieves FE...
Heterogeneous macromolecule catalysts have been known as efficient electrocatalysts for CO2 reduction reaction, however, manipulating the activity of heterogeneous molecules via controllable metal electronic structure is still challenging. Herein, different CO2 activated 3D, robust, nitrogen‐doped hollow carbon spheres are synthesized to anchor cobalt phthalocyanine as molecularly dispersed electrocatalysts,...