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Chiral monolithic silica capillary columns were prepared by immobilization of amylose‐3,5‐dimethylphenylcarbamate (ADMPC) bearing a small fraction of 3‐(triethoxysilyl)propyl residues through intermolecular polycondensation of the triethoxysilyl groups. The obtained columns were used for chiral separations in capillary electrochromatography (CEC). The effects of the silica monolith nature and the...
The 3,5‐dimethylphenylcarbamate derivatives of cellulose bearing 3‐(triethoxysilyl)propyl residues were immobilized in a capillary format onto a monolithic silica support by intermolecular polycondensation of the triethoxysilyl groups. The resulting columns were used for chiral separations using capillary electrochromatography. The effects of the synthesizing solvent, the selector coating procedure,...
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