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Silica packed epoxy networks are prepared in two steps via in situ, solvent free sol–gel processing of tetraethoxysilane in liquid epoxy monomer and curing the mixture with a flexible diamine afterwards. The influence of filler content and processing conditions on the mechanical properties and the fracture behavior is studied by means of the static mechanical analysis and AFM characterization of the...
This paper presents a novel two-stage chronological procedure developed for the synthesis of bicontinuous epoxy–silica hybrid polymers. The epoxy–silica polymers are produced by solvent-free hydrolysis of tetraethylorthosilicate into the liquid epoxy resin, followed by the crosslinking of epoxide groups with a diamine curing agent. The two types of bicontinuous epoxy–silica hybrid polymers prepared...
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