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The incorporation of low-dimensional nanomaterials into 3D metal matrices are promising to translate their intriguing properties from nanoscale to the macroscopic world. However, the design of robust nanofillers and effective fabrication of such bulk composites remain challenging. Here we report a configuration design of nanocarbon for reinforcing metals via unzipping carbon nanotubes (CNTs) into...
In this study, transverse compressive properties of high tensile strength polyacrylonitrile (PAN)-based (T1000GB), high modulus PAN-based (M60JB), high modulus pitch-based (K13D), and high ductility pitch-based (XN-05) single carbon fibers were measured using a direct compression test. The transverse compressive modulus, Ef (TC), of T1000GB, M60JB, K13D, and XN-05 single fibers corresponded to 8.94 GPa,...
Despite significant efforts to develop ways to produce customized carbon-based nanostructures, facile synthesis of mass graphene/graphitic nanoribbons (GNRs) without losing the intrinsic sp2-structure and properties remains challenging. Here we report that bulk of multi-layered graphitic nanoribbons can be prepared by gas-phase oxidative splitting of multi-walled carbon nanotubes (MWCNTs) using HNO...
Low-pressure chemical vapor deposition synthesis of graphene films on two different Cu foils, with different surface oxygen and carbon contents, was performed by controlling H2 and/or Ar flow rates during heating. The influences of heating atmosphere on the final impurity level, quality of the synthesized graphene films and thickness uniformity were investigated depending on Cu foil impurities. Heating...
Wide angle X-Ray scattering was used to measure the progression of alignment when stretching carbon nanotube (CNT) sheets. The nanotubes were grown by an aerogel chemical vapor deposition process and drawn onto a drum rotating at a draw rate of 15 m/min to form a sheet. Samples were cut from this sheet at 0°, 10°, 25°, 45° and 90° with respect to the drawing direction. Samples stretched along the...
Two carbonized oxidized polyacrylonitrile fiber (OPF) felts and one polyacrylonitrile-based carbon fiber (CF) felt were used as preforms to prepare two kinds of carbon/carbon composites by chemical vapor infiltration,and the effect of fiber type on the microstructure and mechanical properties of the composites were investigated. The microstructure was characterized bypolarized light microscopy and...
N-doped activated carbons for electric double-layer capacitors were prepared from waste medium density fiberboard using K2CO3 activation. The effects of carbonization temperature, activation temperature, activation time and K2CO3/coke mass ratios on surface chemical compositions, pore structure and electrochemical performance of the resulting activated carbons were investigated. Results indicated...
Graphene oxide (GO) was found to be a metal-free, water-tolerant and high-efficiency catalyst towards the cycloaddition of carbon dioxide (CO 2 ) to propylene oxide (PO) for the synthesis of propylene carbonate (PC) at room temperature (RT) and atmospheric pressure without the need for a solvent. Using GO as catalyst and tetrabutylammonium bromide (Bu 4 NBr) as co-catalyst, PO is rapidly...
The effect of polyimide coatings on the filament tensile strength of high-strength polyacrylonitrile-based carbon fiber was studied by using dip and high-temperature vapor deposition polymerization (VDP) coating processes. Unlike a VDP on a cold substrate, high-temperature VDP has the potential to directly synthesize and isotropically deposit a polyimide, from diamine and dihydride monomers without...
The thermal conductivities of ultrahigh tensile strength polyacrylonitrile (PAN)-based (T1000GB) and ultrahigh modulus pitch-based (K13D) carbon fibers with carbon nanotubes (CNTs) grown on them using chemical vapor deposition were measured using a thermal diffusivity meter. The thermal conductivities of the resulting hybrid materials were calculated to be 18.6±1.7 and 965.6±30.0W/mK for T1000GB and...
The tensile properties and fracture behavior of ultrahigh tensile strength PAN-based (T1000GB), ultrahigh modulus pitch-based (K13D) and high ductility pitch-based (XN-05) carbon fibers have been investigated. The statistical distributions of the tensile strength were characterized. The Weibull modulus for the T1000GB, K13D and XN-05 fibers were calculated to be 5.9, 4.2 and 7.9, respectively. The...
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