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Core–shell structured Rh 17 S 15 @C and Rh@C nanocomposites have been synthesized by a one-step solvothermal method from the reaction of Rh 6 (CO) 16 with or without sulfur in acetone. The resultant Rh 17 S 15 @C composite consists of spherical Rh 17 S 15 cores with homogeneous diameter of ∼20nm and amorphous carbon shell of 11–15nm in...
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