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New ternary rare earth metal boride carbides with compositions close to RE10B9C10 (RE = Gd, Tb) were prepared from the elements by melting around 1800 K followed by annealing in silica tubes at 1270 K for one month. The crystal structure of the terbium compound was solved by single‐crystal X‐ray diffraction. It crystallizes in a new structure type in the monoclinic space group P21/c, a = 7.937(1),...
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