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New mixed (AlCu)-pillared clays are prepared from a crude bentonite sample (H) (Tunisia deposit) by two discrete procedures: (a) a classical ‘D’ method by which Al or (Al, Cu) nitrate solutions, hydrolyzed with NaOH, are added to a 2% clay suspension and (b) a ‘P’ method where the clay powder is directly dispersed in the pillaring solution. Intercalation reactions are performed at 40°C, with an OH/(Al,...
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