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Palladium film can be deposited on gold polycrystalline electrodes, from a deoxygenated alkaline solution containing 50mM NaOH plus 0.5mM K 2 Pd(CN) 4 . A multipulse sequence of potentials of equal amplitude and duration was used for the palladium deposition process. In particular, an optimized waveform of potentials of E 1 =1.0V vs. SCE and E 2 =−1.0V vs. SCE for the...
A platinum-modified glassy carbon electrode was investigated as an amperometric sensor for the determination of alcoholic species in acidic medium. The described electrode was tested in liquid chromatography and flow-injection analysis by pulsed amperometric detection. It showed a promising combination among catalytic activity, detection limits and reproducibility for the determination of alcoholic...
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