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Redox relationship among anatase, rutile, and a new nonstoichiometric orthorhombic titanium oxide was elucidated. Single crystal of nonstoichiometric orthorhombic titanium oxide TiO 1.94 was prepared by reducing a single crystal of rutile TiO 2 at 950 o C in H 2 for 1h based on this relationship. The single crystallinity was demonstrated by both the Laue...
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