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In this study, we report that geopolymer materials containing different amounts of graphitic carbon nitride (g‐C3N4) (C3N4/GP) can remove methylene blue (MB) using the synergistic effects of adsorption and photodegradation. A geopolymer containing 3 wt% g‐C3N4 (3 wt%C3N4/GP) had the best MB removal efficiency of 94.62% within 60 min, under visible light. The results showed that geopolymers can act...