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β‐In2S3 is a natural defective III–VI semiconductor attracting considerable interests but lack of efficient method for its 2D form fabrication. Here, for the first time, this paper reports controlled synthesis of ultrathin 2D β‐In2S3 flakes via a facile space‐confined chemical vapor deposition method. The natural defects in β‐In2S3 crystals, clearly revealed by optical spectra and optoelectronic measurement,...
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