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Heterogeneous Ru/Re and Rh/Re catalysts, formed in situ from Ru 3 (CO) 12 /Re 2 (CO) 10 and Rh 6 (CO) 16 /Re 2 (CO) 10 respectively, are effective for the liquid phase hydrogenation of cyclohexanecarboxamide (CyCONH 2 ) to CyCH 2 NH 2 in up to 95% selectivity without the requirement for ammonia to inhibit secondary...
Rh/Mo catalysts formed in situ from Rh 6 (CO) 16 and Mo(CO) 6 are effective for the liquid phase hydrogenation of CyCONH 2 to CyCH 2 NH 2 in up to 87% selectivity, without the requirement for ammonia to inhibit secondary amine formation. Use of in situ HP-FTIR spectroscopy has shown that decomposition of metal carbonyl precursors occurs during an extended...
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