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In this paper, we first report the macroporous polyaniline (PANI) microspheres and Ag/PANI core-shell structure via one-pot redox reaction in ethanol at 250°C. Morphology of the obtained products was characterized with scanning electron microscopy (SEM) and transmission electron microscopy (TEM). A series of comparative experiments reveal that both the reaction temperature and AgNO 3 concentration...
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