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Extensive series of tin antimonates were synthesized with a degree of Sn/Sb substitution from 0% to 100%. Metal chlorides were used as starting reagents, and the product materials were precipitated from the liquid phase by raising the pH of the solution using ammonia. The materials were characterized by means of powder X-ray diffractometry and thermogravimetry. The structures of rutile (P4 2 ...
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