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Ionic liquids consisting of N-dodecyl-N-methyl pyrrolidinium bromide [C 12 MPB] in a mixture with D2O, decanol, and DMSO were for the first time found to give anisotropic molecular alignment in magnetic fields and are useful to measure residual dipolar couplings (RDCs) from polar analytes, for example, glucose. The system shows less quadrupolar splitting of the deuterated solvent signal compared...
In the presence of lanthanide cations, some sugars with a special relationship between their hydroxyl groups are able to form complexes in water. Diffusion-ordered NMR spectroscopy (DOSY) can be used as a tool to distinguish between the complexed and noncomplexed forms in a mixture due to the differences in their relative diffusion coefficient values. The lowest diffusion was attributed to the complexed...
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