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We synthesized LiMnPO4/C with an ordered olivine structure by using a microwave-assisted polyol process in 2:15 (v/v) water–diethylene glycol mixed solvents at 130°C for 30min. We also studied how three surfactants—hexadecyltrimethylammonium bromide, polyvinylpyrrolidone k30 (PVPk30), and polyvinylpyrrolidone k90 (PVPk90)—affected the structure, morphology, and performance of the prepared samples,...
LiNi 0.5 Mn 1.5 O 4 was synthesized by combustion synthesis (UCS) using urea as fuel. X-ray diffraction and scanning electron microscope measurements showed that the spinel structure LiNi 0.5 Mn 1.5 O 4 with the space group Fd3¯m was formed during urea combustion. Both structure and particle size could be adjusted by the amount of urea and the heat treatment...
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