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Vibration spectral properties and dehydration behaviors of goethite nanorods with diameters ranging from 13 to 32 nm were investigated using infrared spectroscopy, thermogravimetric analysis, and X-ray diffraction. All goethite nanorods were highly hydrated with physisorbed and chemisorbed water. As the diameters of goethite nanorods increased, the hydroxyl deformation vibration in the a-b plane showed...
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