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XPS and metathesis activity studies were performed on oxidic allyl‐based Mo/SiO2 catalysts (0.5 wt% Mo) and the oxidic catalyst following photoreduction to various extents. XPS results and average oxidation state measurements from the amount of CO2 formed during photoreduction, indicated that controlled photoreduction of the oxidic catalyst, in CO atmosphere, produces a mixture of Mo6+ and Mo4+ oxidation...
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