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Two hybrids, [BMIP][Pb2Cl6] (1) and [BMIP][Pb1.5Cl5]·H2O (2) {BMIP2+ = 1,3‐bis(1‐methylimidazolium)propane}, are achieved by mutual diffusion of inorganic and organic components in anhydrous DMF and DMF with a trace amount of water (the trace amount of water originates from MnCl2·4H2O), respectively. Single‐crystal X‐ray diffraction data are collected for 1 in 300–100 K and 2 in 370–100 K, revealing...
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