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A method for the synthesis of phosphabenzenes under iron catalysis is described. Thus, the FeI2‐catalyzed [2+2+2] cycloaddition of diynes with phosphaalkynes in m‐xylene gave a variety of phosphabenzenes in good to high yields (up to 87 % yield).
The NN bond of molecular dinitrogen bridging two molybdenum atoms in the pentamethylcyclopentadienyl molybdenum complexes that bear ferrocenyldiphosphine as an auxiliary ligand is homolytically cleaved under visible light irradiation at room temperature to afford two molar molybdenum nitride complexes. Conversely, the bridging molecular dinitrogen is reformed by the oxidation of the molybdenum nitride...
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