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A novel diiron S-(−)-1-phenylethylazadithiolate complex, Fe2[(μ-SCH2)2NCH(CH3)Ph](CO)6 (1), has been prepared by the condensation of Fe2(μ-SH)2(CO)6, CH2O and S-(−)-1-phenylethylamine. Furthermore, the reaction of complex 1 and phosphine ligands (PPh3, P(C6H4-4-F)3, dppe) in the presence of the decarbonylation agent Me3NO·2H2O resulted in the formation of the phosphine-substituted diiron S-(−)-1-phenylethylazadithiolate...
Three novel diiron azadithiolate complexes Fe2[(μ-SCH2)2NCH2CH2CH(CH3)2](CO)6 (1), Fe2[(μ-SCH2)2NCH(CH2CH3)2](CO)6 (2) and Fe2[(μ-SCH2)2NCH2CH2CH2SCH3](CO)6 (3) have been synthesized by treatment of Fe2(μ-SCH2OH)2(CO)6 with primary amines RNH2 (R=CH2CH2CH(CH3)2, CH(CH2CH3)2, CH2CH2CH2SCH3). Meanwhile, reaction of Fe2(μ-SCH2OH)2(CO)6 and diphosphine ligand Ph2PCH2PPh2 (dppm), followed by the addition...
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