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Sequence‐controlled polymerization is the forefront of polymer chemistry. Herein, the feasibility of sequence regulation by using organocatalyzed ring‐opening polymerization (ROP) is demonstrated. In particular, ring expansion strategy is employed to synthesize pre‐organized monomers 1 and 2. ROP is conducted by using 1,5,7‐triazabicyclo[4.4.0]dec‐5‐ene and benzyl alcohol as the catalyst and initiator,...
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