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Iridium submicroparticles (SMPs) were prepared at room temperature via a photochemical reduction route in aqueous solution with polyvinylpyrrolidone (PVP) as capping agent. We found that the incident wavelength has a great effect on the growth rate of Ir SMPs. The shorter the wavelength is, the faster the generation of Ir SMPs is. The Ir SMPs were composed of the Ir nanoparticles (NPs), showing discus-like...
A novel electrochemical method for the determination of sulphide at a multi-walled carbon nanotube-dihexadecyl hydrogen phosphate composite film coated glassy carbon electrode (MWNTs-DHP/GCE) based on in situ synthesis of methylene blue (MB) was established.
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