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In this work, the effects of preparation conditions used in roughening silver substrates by electrochemical triangular-wave oxidation–reduction cycles (ORC) on surface-enhanced Raman scattering (SERS) were first investigated. The optimum roughening conditions for obtaining strongest SERS of Rhodamine 6G (R6G) are as follows. Ag electrodes were cycled in deoxygenated aqueous solutions containing 0...
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