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Efficient and economical separation of 1,3‐butadiene (C4H6) from C4 hydrocarbons is imperative yet challenging in industrial separation processes. Herein, a guest‐induced flexible Mn‐bpdc metal–organic framework (MOF) has been employed to separate C4H6 from C4 hydrocarbons, including n‐butene (n‐C4H8), iso‐butene (iso‐C4H8), n‐butane (n‐C4H10), and iso‐butane (iso‐C4H10). Significantly, C4H6 can instantaneously...
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