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A strategy for in situ fabrication of nanoscale‐thin layers of anatase TiO2 coated on the metal–organic framework (MOF) material, MIL‐53(Al), is developed. The preparation conditions for crystallized TiO2 are normally incompatible with the thermal and chemical stability of MOFs. Based on our strategy, we found that the redundant organic ligands (1,4‐benzenedicarboxylic acid, H2BDC) within the pores...
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