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In order to prepare ZrC-ZrB2 nanocomposite ceramics with high temperature stability from single-source precursors, the reactions of ZrCl4, allyl amine, allyl-MgCl and borane were employed to synthesize suitable precursors. The meliorated ZrNCB precursor had favorable solubility and higher ceramic yield (68.8wt%), which was then transformed to ZrC-ZrB2 ceramics at different temperatures. The main phase...
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