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A novel Cd II -coordination framework [Cd(C 4 O 4 )(btb)(H 2 O) 2 ] n (1) constructed by squaric acid (H 2 C 4 O 4 ) and secondary N-donor spacer 1,4-bis(1,2,4-triazol-4-yl)butane (btb) is presented, which displays 2D→3D inclined polycatenate framework consisting of two of sets of equivalent 2D 4 4 -sql layers and (4,6)-connected...
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