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A novel platinum cavity electrode (Pt-CE) was fabricated by drilling a small circular cavity (0.5mm diameter) through a thin Pt foil (ca. 0.15mm thickness, 2.0mm width). It was used to record cyclic voltammograms (CVs) of the insulative AgCl powder (as a model) in aqueous solutions. The voltammetric response of the electrode was fast (tested to 100mV/s) and the charge under the reduction peak agreed...
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