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Two Keggin polyoxometalate (POMs) based hybrid compounds containing helix/nanocages as peroxidase-like mimics have been synthesized and structurally characterized. Single crystal X-ray diffraction analysis reveals that compound 1 exhibits a POM-pillared framework with open nanotube channels (ca. 5.6 × 5.8 Å2), in which SiW12 polyanions are sandwiched between the adjacent Cu-fkz sheets with meso-helix...
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