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In this study we developed a novel synthesis called "ferrite route," by which we can fabricate Fe nanoparticles larger than 10 nm at a yield 10 times higher than that obtained by the above mentioned methods. Synthesis is made at 90degC, without using any hazardous materials. We found that the Fe nanoparticles via the ferrite route were more easily embedded in poly-glycidyl methacrylate (poly-GMA),...
The novel "ferrite route" was developed for synthesis of iron nanoparticles. Precursor Fe3O4+delta nanoparticles were synthesized by coprecipitation oxidation from aqueous solutions of xFeCl2 +(1-x)/FeCl3 (0lesxles1), which were reduced by hydrazine at 90degC. Under optimum conditions of x=0.66, the iron nanoparticles were 15plusmn3.7 nm in diameter and had a saturation magnetization of...
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