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Durch CuCl‐vermittelte Insertion von Indium in Alkylhalogenide wurden Alkylindiumreagentien erzeugt und unter Palladiumkatalyse mit Arylhalogeniden gekuppelt (siehe Schema). Die Reagentien sind mit verschiedenen funktionellen Gruppen verträglich und daher von allgemeinem Nutzen für organische Synthesen. DMA=N,N‐Dimethylacetamid, TBS=tert‐Butyldimethylsilyl.
A direct result: Alkyl indium reagents are synthesized by the insertion of indium into alkyl halide mediated by CuCl. The synthetic utility of these reagents is demonstrated by their palladium‐catalyzed coupling with aryl halides (see scheme). The reagents are compatible with various functional groups, and this makes the protocol generally useful in organic synthesis. DMA=N,N‐dimethylacetamide, TBS=...
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