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A confirmed structure of meroterpenoid myrtucommulone K, which is vastly different from the originally reported one, is conducted. The first biomimetic total synthesis towards the assignment of its absolute configuration has been efficiently accessed in 5 steps, and key to the success was a heteroatom Diels-Alder cycloaddition. The structure of myrtucommulone K was re-elucidated and confirmed by extensive...
A novel m-terphenyl-based steric protection group (Bpq group) bearing a dendrimer-type framework was designed and successfully applied to the stabilization of the corresponding N-thiosulfinylaniline and arenesulfenyl iodide. The Bpq group was found to provide a very inert environment for the reactive functionality embedded in its cleft.
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