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High‐quality double‐shelled TiO2 hollow spheres (DHS‐Ti) assembled with TiO2 nanosheets have been synthesized for the first time through a simple hydrothermal treatment of sSiO2@TiO2 (TiO2‐coated solid SiO2 spheres). The double‐shelled structure shows a high BET surface area up to 417.6 m2 g−1. Anatase DHS‐Ti of high crystallinity can be obtained without structural collapse by calcination treatment...
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