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Improving the dimensional stability is significant for fluorinated poly(aryl ether) (FPAE). In this work, zirconium tungstate (ZrW2O8) with negative thermal expansion (NTE) modified by thiol groups is successfully obtained by surface modification with 3‐(trimethoxysilyl)‐1‐propanethiol. Then, the dispersion of ZrW2O8 is improved and a certain crosslinked structure is formed by click reaction between...
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