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A novel hydrophobic rare earth‐based aluminum hypophosphite (AHP) was prepared using rare earth aluminate coupling agent (REA) in a ball mill with a one‐step mechanochemistry method, and used as flame retardant for epoxy resin. It has been found that RaAHP‐4 (AHP was modified by 4 wt% REA) exhibited excellent hydrophobic properties with the water contact angle of 94.58°. The effect of RaAHP‐2 (AHP...
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