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In this work, a novel enantioselective MCE was developed employing BSA‐conjugated Fe3O4@Au nanoparticles (Fe3O4@Au NPs) as stationary phase. Fe3O4@Au NPs with high magnetic responsively, excellent solubility, and high dispersibility in water were prepared through a sonochemical synthesis strategy. BSA was then immobilized onto the Fe3O4@Au NPs surfaces through the well‐developed interaction between...
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